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Triplex‐forming peptide nucleic acids (TFPNAs) were targeted to double‐helical regions of 19F‐labeled RNA hairpin models (a UA‐rich duplex with a hexaethylene glycol (heg) loop and a microRNA model, miR‐215). In addition to conventional UV‐ and circular dichroism (CD)‐based detection, binding was monitored by 19F NMR spectroscopy. Detailed information on the stoichiometry and transition between the...
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