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The ultraviolet laser desorption/ionization of polyaromatic hydrocarbons (PAHs) has been investigated under different background pressures of an inert gas (up to 1.2 mbar of N2) in the ion source of a hybrid, orthogonal‐extracting time‐of‐flight mass spectrometer (oTOF‐MS). The study includes an ensemble of six model PAHs with isolated single polyaromatic cores and four ones with multiple cross‐linked...
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