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Nanostructured materials can exhibit phase change behavior that deviates from the macroscopic phase behavior. This is exemplified by the ambiguity for the equilibrium phases driving the first open‐circuit voltage (OCV) plateau for the lithiation of Fe3O4 nanocrystals. Adding complexity, the relaxed state for LixFe3O4 is observed to be a function of electrochemical discharge rate. The phases occurring...
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