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The kinetic performance of 0.5mm×50mm columns packed with 2.7μm Halo-C 18 core–shell particles and 3μm EP-120-C 18 fully porous particles fitted on an Eksigent LC-Express Ultra μHPLC system were measured. The instrument contribution to band broadening was obtained by directly connecting the injection valve and the detector cell with a short, narrow PEEKSIL tube. The connections between...
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