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Monolithic capillary columns were prepared by copolymerization of styrene and divinylbenzene inside a 200μm i.d. fused silica capillary using a mixture of tetrahydrofuran and decanol as porogen. Important chromatographic features of the synthesized columns were characterized and critically compared to the properties of columns packed with micropellicular, octadecylated poly(styrene-co-divinylbenzene)...
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