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The influence of synthesis conditions on morphology and structure of CeO2 nanocrystals prepared by microwave‐assisted hydrothermal method were studied by XRD, TEM, Raman spectroscopy and photoluminescence measurements. Decisive effect of the OH‐/Ce3+ molar ratio in the reaction mixture on the size and shape of CeO2 nanocrystals was established and explained. Rise of the concentration of OH‐ groups...
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