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Silicalite-1 has been hydrothermally synthesized in a bicontinuous microemulsion of tetraethylenepentamine–sodium bis(2-ethylhexly) sulfosuccinate (AOT)–water system containing fluoride ions. The presence of AOT (an anionic surfactant) has been found to be essential for the formation of Silicalite-1 in bulk tetraethylene pentamine solvent. The tetrahedral binding sites of silicon atom have been confirmed...
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