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The use of inelastic neutron scattering (INS) spectroscopy has allowed the determination of the infrared and Raman inactive out-of-plane bending mode ν 5 in the [PdCl 4 ] 2- ion at 136 cm -1 . To our knowledge, this is the first time this mode has been observed in any homoleptic square planar complex. An initial highly anomalous INS spectrum was shown by the...
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