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Discrete organoimide complexes of the divalent rare‐earth metals samarium, europium, and ytterbium are reported. Tandem salt metathesis‐protonolysis reactions using LnII bis(tetramethylaluminate) precursors [Ln(AlMe4)2]n and monopotassium salts of 2,6‐diisopropylaniline (H2NDipp) and triphenylsilylamine prove viable and efficient protocols. Depending on the ionic radius of the LnII metal centers and...
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