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Well-shaped Rh particles grown epitaxially on NaCl surfaces were coated with a 25 nm layer of crystalline vanadium oxide by reactive deposition in 10 −4 mbar oxygen. The Rh/VO x film was subjected to consecutive heat treatments in 1 bar oxygen and in 1 bar hydrogen up to 673 K. The structural and morphological changes were monitored by (high-resolution) transmission electron microscopy,...
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