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Halogen bonding between two negatively charged species, tetraiodo‐p‐benzoquinone anion radicals (I4Q−.) and iodide anions, was observed and characterized for the first time. X‐ray structural and EPR/UV–Vis spectral studies revealed that the anion–anion bonding led to the formation of crystals comprising 2D layers of I4Q−. anion radicals linked by iodides and separated by Et4N+ counter‐ions. Computational...
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