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A quenchable new high‐pressure–high‐temperature modification of antimony(III) oxide, γ‐Sb2O3, has been obtained at hydrostatic pressures of 9–11 GPa and temperatures of 573–773 K. Its crystal structure has been determined from high‐resolution synchrotron powder diffraction data. γ‐Sb2O3 consists of three‐dimensionally cross‐linked infinite chains of SbO3E units (E = lone pair) with the chains forming...
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