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Ag 3 Ni 2 O 4 was obtained as single crystals from a mixture of 2H–AgNiO 2 and Ag 2 O in oxygen high-pressure autoclaves (P6 3 /mmc (no. 194), a=2.9331(6), c=28.313(9)Å, Z=2). It may be regarded as a stage-2 intercalation compound of the host 2H–AgNiO 2 and is the first staging compound constituted of alternating subvalent ∞2Ag2+ and Ag +...
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