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The kinetics of oxidative addition of CH 3 I to [Rh(FcCOCHCOCF 3 )(CO)(PPh 3 )], where Fc=ferrocenyl and (FcCOCHCOCF 3 ) − =fctfa=ferrocenoylacetonato, have been studied utilizing UV/Vis, IR, 1 H and 31 P NMR techniques. Three definite sets of reactions involving isomers of at least two distinctly different classes of Rh III -alkyl and...
The synthesis of a variety of tetrahedral β-diketonato titanium(IV) complexes of the type [(C5H5)2Ti(CH3COCHCOR)]+ClO4- with R=CF 3 , OCH 3 , C 6 H 5 , CH 3 and Fc is described. The Ti III /Ti IV couples and the Fc/Fc + couple exhibited chemically and electrochemically reversible cyclic voltammetric behaviour. The formal reduction potential...
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