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A series of Ag/Zn–Al layered double hydroxide composites were successfully synthesized by a mechanochemical method, and their photocatalytic activity as methyl orange (MO) degradation was investigated. The nanoscale composites showed excellent photocatalytic activity and enabled simply over 95% degradation of MO under visible light irradiation in 180 min. Based on the results from EIS and PL analyses,...
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