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Two series of boronium‐cation‐based ionic liquids were prepared and fully characterized by 1H, 13C, and 11B NMR and infrared spectroscopy, differential scanning calorimetry (DSC), and elemental analysis. The structure of bis(1‐methyl‐1H‐imidazole‐3‐yl)dihydroboronium dicyanoborohydride (5 a) was determined by single‐crystal X‐ray diffraction. The densities of these ionic liquids range from 1.05 to...
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