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The main aim of this work is to obtain heterogeneous, zirconocene aluminohydride/methylaluminoxane (MAO) polymerization catalysts, without using inorganic carriers like silica. The syntheses of zirconocenium ion‐based clathrates, formed from aluminohydride zirconocene complexes activated with MAO, are reported here. Several different approaches were examined for the synthesis of these clathrate compositions;...
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