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A novel CsF-catalyzed three-component coupling reaction of a silylphosphine, activated alkenes and aldehydes is described. Multi-functional phosphines were obtained by forming both carbon–phosphorus and carbon–carbon bonds in good yields under mild conditions.
Regioselective phosphination of carbon–carbon unsaturated bonds by a fluoride-mediated reaction of silylphosphines is described. Alkenes and alkynes having a directing group, such as an aromatic or a carbonyl group, reacted to form a carbon–phosphorus bond under mild conditions. When an anhydrous fluoride source was applied in the presence of an electrophile, the corresponding three-component coupling...
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