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Superstructured microspheres were prepared via a two-tier hierarchical assembly of a fluorine-containing diblock copolymer, poly(tert-butyl acrylate)-b-poly(2-[(perfluorononenyl)oxy]ethyl methacrylate) (PtBA-b-PFNEMA) with well controlled block lengths. At tier 1, water induced self-assembly of the diblock copolymer produced nanospheres of low dispersity with onion-like multilayer inside structures,...
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