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Single-crystalline TiOF 2 nanocubes with edge length of around 200–300nm have been synthesized under hydrothermal conditions using titanium (IV) isopropoxide (TIP) as titanium source, HF as etchant. The corresponding hollow TiO 2 nanocages with dominantly exposed {001} crystal planes can be easily obtained by calcinating TiOF 2 nanocubes under air atmosphere. It is also found...
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