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Mechanisms of C3–C4 alcohol synthesis from syngas are elucidated over a Mg/Al mixed metal oxide (MMO) supported K/MoS2 catalyst via 13C2-ethanol and 13C2-ethylene co-feeds. K/bulk-MoS2 is used as a control catalyst to provide insight into the role of K/MoS2 and K/MoS2-MMO sites on higher alcohol formation pathways. Analysis of the products via 13C NMR show preferential enrichment of terminal carbons...
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