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Solvothermal reactions of CuX (X = Cl, Br, I, CN) with bis(4‐iodo‐1H‐pyrazol‐1‐yl)methane (ipzm) or its methyl‐substituted derivative bis(4‐iodo‐3, 5‐dimethyl‐1H‐pyrazol‐1‐yl)methane (idmpzm) resulted in the formation of three 2D [Cu2X2]n‐based coordination polymers [{Cu(μ‐X)}2(μ‐ipzm)]n [X = Cl (1), Br (2), I (3)], four 1D [CuX]n‐based coordination polymers [{Cu(μ‐CN)}2(μ‐ipzm)]n (4), [{(idmpzm)Cu}(μ‐Cl)]...
One novel Cu(II)-Fe(III) heteronuclear complex [Cu2(oxen)Fe(CN)5(NO)]n (H2oxen = N,N'-bis(2-aminoethyl)oxamide) was synthesized by the reaction of Cu(oxen)·2H2O with Cu(ClO4)2·6H2O and Na2[Fe(CN)5NO]·2H2O. The crystal structure was determined by single-crystal X-ray diffraction. The complex crystallizes orthorhombic with space group Pnma, and forms a centrosymmetric Cu(II)-Fe(III) heteronuclear molecule...
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