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A new two‐dimensional tetrathienyl‐TBDT (TBDT‐4T) was synthesized by employing palladium‐catalyzed C─H benzannulation between an iodobiaryl and 1,2‐dithienylacetylene. The stannylated TBDT‐4T was copolymerized with di(thiophenyl)difluorobenzothiadiazole (FBT) and fluorothienothiophene (FTT) monomers to yield PTBDT‐FBT and PTBDT‐FTT, which showed high decomposition temperatures (421 and 408°C) and...
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