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Metallic palladium (Pd) electrocatalysts for oxygen reduction and hydrogen peroxide (H2O2) oxidation/reduction are prepared via electroplating on a gold metal substrate from dilute (5 to 50 mM) aqueous K2PdCl4 solution. The best Pd catalyst layer possessing dendritic nanostructures is formed on the Au substrate surface from 50 mM Pd precursor solution (denoted as Pd‐50) without any additional salt,...
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