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A novel strategy for the synthesis of 2‐substituted thioglycals has been developed from a carbohydrate‐derived ketene dithioacetal in a two‐step sequence. The introduction of various electrophilic groups at the double bond of the ketene dithioacetal was achieved before the elimination of the thioalkyl group to yield 2‐substituted thioglycals. Removal of the exocyclic thioalkyl group was obtained by...
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