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The reaction of the half-open titanocene Ti(C 5 H 5 )(c-C 8 H 11 )(PMe 3 ) (c-C 8 H 11 =cyclooctadienyl) with four equivalents of PhC 2 SiMe 3 has been found to lead to an unusual, very electron deficient coupling product, containing both metallacyclobutane and metallacyclobutene fragments. Structural studies of both complexes...
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