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Various materials of the formulas Mo 3−x Fe x Sb 7 and Mo 2.6 Fe 0.4 Sb 7−y Te y have been prepared by solid state synthesis at 873K, starting from the elements in the stoichiometric ratios. The Fe content can be as high as x=0.45, while attempts to incorporate 0.5 Fe lead to the formation of FeSb 2 as a minor side product. At x=0.4,...
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