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The unsaturated vicinal phosphane/borane frustrated Lewis pairs (P/B FLPs) Ph2PC(p-tolyl)=C(R)B(C6F5)2 (R=C6F5 or CH3) react with tert-butyl isocyanide to give an equilibrium mixture of the starting materials, the borane/isonitrile adduct and the P/B addition product to the isonitrile carbon atom. The cooperative 1,1-adducts were exclusively formed upon treatment of these FLPs with n-butyl isocyanide...
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