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The construction of high‐performance MOF‐based hollow fiber composite membrane (HFCM) modules is a significant, yet challenging task for the biofuel production industry. In this study, a novel approach was taken to fabricate PDMS@ZIF‐8/PVDF HFCMs in modules through a facile ZIF‐8 self‐crystallization synthesis followed by pressure‐assisted PDMS infusion for pervaporation ethanol‐water separation....