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The water–gas shift (WGS) reaction on co-precipitated NiO–ZnO catalysts at different reduction temperatures has been studied by a temperature-programmed reaction using in situ diffuse reflectance infrared Fourier Transform Spectroscopy, coupled with mass spectroscopic (in situ DRIFTS/MS) techniques. The results reveal that a catalyst reduced at 493 K (labeled H220) showed higher activity than one...
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