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The first example of a formal 1,3‐B−H bond addition across the M−N≡N unit of an end‐on dinitrogen complex has been achieved. The use of Piers’ borane HB(C6F5)2 was essential to observe this reactivity and it plays a triple role in this transformation: 1) electrophilic N2‐borylation agent, 2) Lewis acid in a frustrated Lewis pair‐type B−H bond activation, and 3) hydride shuttle to the metal center...
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