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The structural properties of the hydrated lanthanoid(III) ions in aqueous solution and in the isostructural trifluoromethanesulfonate salts have been investigated by a quantitative analysis of the X‐ray absorption near‐edge structure (XANES) spectra at the K‐ and L3‐edges. The XANES analysis has provided a clear description of the variation of lanthanoid(III) hydration properties across the series...
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