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Crystal structures of MgCoGa, Mg0.74CoGa0.52 and Mg0.49CoGa0.15 phases from the Mg–Co–Ga system were investigated using single‐crystal diffraction. These structures belong to the family of so‐called Laves phases. Hexagonal MgCoGa crystallizes as a disordered phase within the MgZn2 structure type. The orthorhombic structure of Mg0.74CoGa0.52 is a distortion variant of MgZn2 and URe2 structure type,...