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A thermal oxide scale has been grown on a high-chromium iron-nickel alloy under very low oxygen partial pressure (1050°C, 10−10Pa). In this paper, a special attention has been paid to morphological and chemical characterizations of the scale by scanning transmission electron microscopy and energy dispersive X-ray analysis at high resolution on a cross-section thin lamella beforehand prepared by using...
The present work is focused on the oxidation at 1050°C of a model chromia-forming alloy, paying special attention to the control of the oxygen partial pressure. Taking benefit of a recently developed approach to describe and fit photocurrent energy spectra, photoelectrochemical characterizations allowed to reveal the presence, in the scale formed at low P(O2) (10−15atm), of an unexpected high number...
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