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A pair of enantiopure cubane‐type CuII4O4 clusters was constructed from simple chiral ligands (R or S)‐2‐[(2‐hydroxy‐1‐phenylethylimino)methyl]phenol (H2LR or S). Single‐crystal X‐ray diffraction studies demonstrated that complexes 1R and 1S are enantiomers. They consist of a CuII4O4 cubane core in which the four CuII centres are linked by a μ3‐oxo bridge. The four CuII ions in one cluster are all...
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