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Stable α-MnS spheres have been successfully synthesized by two-step solvothermal method and traditional solvothermal technique without any surfactant assistance. The XRD patterns and FE-SEM images show that the as-prepared samples are cubic α-MnS micro-spheres with different morphologies. The formation of spheres was studied under different experimental conditions. The two-step solvothermal method...
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