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The red-violet nickel (II) complex [Ni (C 8 H 18 N 4 O 2 ) (NO 2 ) 2 ]·H 2 O (3) was synthesized from an aqueous solution containing nickel chloride, sodium nitrite and 4,7-diazadecanediamide (1). The NO 2− ions in compound 3 are bound to the metal center through the nitrogen atoms. On heating the solid sample of compound 3, the...
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