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A series of molybdenum phosphide catalysts with initial Mo/P ratios varying in a narrow range of 0.90–1.10 was prepared by temperature-programmed reaction; characterized by X-ray diffraction, BET, elemental analysis, X-ray photoelectron spectroscopy, and CO chemisorption measurements; and tested for the hydrogenation of acetonitrile at different pressures (0.1–1.0 MPa) and temperatures (473–513 K)...
A series of molybdenum phosphide catalysts were prepared from initial Mo/P molar ratios ranging from 0.6 to 2.6. The catalytic activity of the catalysts for the selective hydrogenation of acetonitrile was studied. The catalysts with initial Mo/P ratios > 1.0 have high selectivity for ethylamine (80%–90%), and for the catalysts with Mo/P ratios < 1.0, the selectivity for diethylamine and triethylamine...
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