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A manganese‐catalyzed regioselective ring‐opening peroxidation of cyclobutanols has been disclosed. With this protocol, the C(sp3)−OOBu‐t bond could be efficiently constructed via the radical‐mediated C−C bond cleavage/coupling, allowing the facile access to a variety of 4‐oxo peroxides. Besides, the obtained peroxidation products could be readily transformed into other synthetically attractive skeletons...
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