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Lead nanoparticles ranging from 10-200 nm were prepared by reacting [Pb{N(SiMe 3 ) 2 } 2 ] with the reducing agent tert-butoxy alane, [H 2 Al(OtBu)] 2 , in non-aqueous media. By this reaction, Pb nuclei on the molecular scale can be produced imparting a high regularity of shape and size to the resulting nanoparticles. The amino-alkoxo-alane {[(Me 3 Si)...
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