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LiAlH4 and AlCl3 reacted in a ratio 1:3 to obtain Cl2AlH, which is stabilised by the addition of two equivalents of N‐methylpiperidine (nmp) to form dichloroalane (1) as bis adduct of nmp. Compound 1 was allowed to react with 2,6‐tBu‐4‐MeC6H2OH and HOcHex in a 1:1 ratio to get compounds 2 and 3, respectively. Cl2Al(2,6‐tBu‐4‐MeC6H2O)(nmp) (2) is a monomer in which the central aluminium atom is tetracoordinate...
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