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In this work, mesoporous NiO with three-dimensional flowerlike morphology were synthesized from precursor α-Ni(OH)2 by a facile template-free modified homogeneous precipitation method, where CO(NH2)2 could be acted as a chelating agent at lower temperatures, and source material of OH− utilizing the hydrolysis reaction at high temperatures. The structures of the NiO materials were characterized by...
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