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Four novel crystalline stereocomplexed polymers are formed by mixing isotactic (R)‐ and (S)‐polycarbonates in 1:1 mass ratio. They show the enhanced thermal stability and new crystalline behavior, significantly distinct from the component enantiomer. Two stereocomplexed CO2‐based polycarbonates from meso‐3,4‐epoxytetrahydrofuran and 4,4‐dimethyl‐3,5,8‐trioxabicyclo[5.1.0]octane have high melting temperatures...
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