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The chemistry of 2‐phosphaethynolate is burgeoning, but there remains much to learn about this ligand, for example its reduction chemistry is scarce as this promotes P‐C‐O fragmentations or couplings. Here, we report that reduction of [U(TrenTIPS)(OCP)] (TrenTIPS=N(CH2CH2NSiPri3)3) with KC8/2,2,2‐cryptand gives [{U(TrenTIPS)}2{μ‐η2(OP):η2(CP)‐OCP}][K(2,2,2‐cryptand)]. The coordination mode of this...
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