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Kaliumacyltrifluorborate (KATs) sind schwer zu synthetisieren, im Bild symbolisiert durch Personen, die mühevoll einen Berg besteigen. H. Ito et al. präsentieren in ihrer Zuschrift auf S. 7377 eine zweistufige KAT‐Synthese aus Aldehyden über eine sequenzielle CuI‐katalysierte Borylierung und Oxidation, die viel einfacher und schneller als herkömmliche Methoden ist. Diese atomökonomische Methode wird...
Potassium acyltrifluoroborates (KATs) were prepared through copper(I)‐catalyzed borylation of aldehydes and subsequent oxidation. This synthetic route is characterized by the wide range of aldehydes accessible, favorable step economy, mild reaction conditions, and tolerance of various functional groups, and it enables the facile generation of a range of KATs, for example, bearing halide, sulfide,...
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