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Fe nanoparticles immobilized on polyaniline-covered carbon nanotube (CNT) surfaces (Fe NPs–PANI/CNT) are prepared by reducing FeCl3 in the mixing solution of aniline and CNT. Significantly, the structure of such composites can be effectively optimized by pretreating FeCl3 with sodium citrate (CA). In the absence of CNTs, we found these two routes have large differences in reduction behaviors and different...
This paper established an in-situ synthesis strategy that the mixing solution of aniline, CNTs and CoCl 2 was directly reduced to prepare polyaniline-cobalt-carbon nanotube (PANI-Co-CNT) electrocatalyst. Furthermore, this strategy was effectively modified by pretreating CoCl 2 precursor with citric acid (CA), forming 2-4nm cobalt nanoparticles uniformly distributed on PANI-CNT support...
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