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Nanocrystalline SiBCN monoliths with the same Si/C/N mole ratio and various boron additions ranged from 0 to 3.0mol were prepared by mechanical alloying plus reactive hot pressing methods. Correction of boron content and microstructural/morphological evolution was investigated in detail by XRD, SEM, TEM and STEM-EDX structure characterization. Except for SiC and BN(C), boron addition contributes to...
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