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The engineering and tailoring of porous materials to realize the precise discrimination of CO2 and C2H2, with almost identical kinetic diameters, is a challenging task. We herein report the first example of the kinetic‐sieving of relatively larger molecule of C2H2 from CO2 by a novel sulfonic anion‐pillared hybrid ultramicroporous materials of ZU‐610a. Specifically, ZU‐610 constructed from copper(II),...
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