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A highly electron‐deficient C3‐symmetric tris(bipyridyl) ligand was prepared in four steps and used for the coordination of Fe(OTf)2, thereby resulting in the homochiral assembly of a new family of robust tetrahedral M4L4 cages. This homochiral T‐symmetric cage containing a relatively large cavity of 330 Å3 is capable of encapsulating an anionic guest, as was determined by mass spectrometry, 19F NMR...
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