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Tridentate PSiP pincer ligands featuring two phosphine donors and an anionic Si donor have attracted considerable attention in recent years. Here, we report the synthesis of the η3-cyclooctenyl complex, (PhPSiP)Ni(η3-cyclooctenyl) (1; PhPSiP=Si(Me)(2-PPh2–C6H4)2) through the reaction of Ni(COD)2 with PhPSiHP (PhPSiHP=HSi(Me)(2-PPh2–C6H4)2). We propose, that as a result of β-hydride elimination of...
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